Determination of histamine in tomatoes by liquid chromatography/mass spectrometry.
نویسندگان
چکیده
The histamine level in tomato fruits and pastes was determined by 2 orthogonal techniques as a means of comparing accuracy. Close statistical agreement was found between assays for free histamine by capillary electrophoresis (with UV absorbance detection), and for the dansyl derivative by reversed-phase liquid chromatography (LC). Both techniques have adequate sensitivity for the analysis of endogenous histamine in tomatoes, but LC/electrospray tandem mass spectrometry was more sensitive by at least an order of magnitude, down to a level of 0.05 mg/kg.
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عنوان ژورنال:
- Journal of AOAC International
دوره 83 3 شماره
صفحات -
تاریخ انتشار 2000